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- W2487101553 abstract "For the first time, we experimentally detected the formation of 6-fold symmetry patterned microcrystals of AlN (aluminum nitride), such as simple prisms, stellar and sectored plates, and stellar and fernlike stellar dendrites. These crystals were formed during combustion of a solid mixture of Al + kAlF3 (k = 0.05–0.1 mol) under a nitrogen atmosphere (PN2 = 2.5 MPa). The combustion temperature recorded with a thermocouple was in the 1700–1900 °C range. We examined the physical mechanisms governing the formation of AlN crystals, and we treated this problem as a case study of the dynamics of crystal growth from the liquid phase. Particular attention was given to the basic theoretical understanding of the subject, utilizing first-principles density functional theory calculations. The Wulff construction method was applied to identify equilibrium structures of nano- and microscale AlN crystals. Energy minimization arguments were used to show that certain crystal planes of AlN are more probable than others, giving the crystal 6-fold symmetry. The integrated experiments and computations form the basis for our proposal of the underlying mechanisms for nucleation and growth of the AlN crystals." @default.
- W2487101553 created "2016-08-23" @default.
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- W2487101553 date "2016-07-29" @default.
- W2487101553 modified "2023-10-09" @default.
- W2487101553 title "Experimental Growth of New 6-fold Symmetry Patterned Microcrystals of AlN: Equilibrium Structures and Growth Mechanism" @default.
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- W2487101553 doi "https://doi.org/10.1021/acs.cgd.6b00829" @default.
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