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• W2487619324 abstract "The analysis of complex mixtures particularly requires the combination of both separation techniques and mass spectrometry. [1-3] The first step in this direction was made by gas clzromatofJraphy-mass .Ipectrometry coupLinfJ (GC-MS), [4] and soon, GC-MS became a routine method. [5-7] The desire to realize a liquid chro­ matofJraphy-mass spectrometry coupling (LC-MS) [8,9] was the driving force for the development of API methods (Chap. 11). [10-13] Coupling of other liquid phase separation techniques to mass spectrometry followed: capillary zone elec­ trophoresis-mass spectrometry (CZE-MS), [14-18] and supercritical fluid chro­ ma{()fJraphy-mass spectrometry (SFC-MS). [19-23] Whatever the separation tech­ nique, it adds an additional dimension to the analytical measurement. The hyphen used to indicate the coupling of a separation technique to mass spectrometry led to the term hyphenated methods. However, mass spectrometry itself offers two additional degrees of freedom. One can either resolve the complexity of a sample by going to high or even ultra­ high mass resolution or one can employ tandem MS techniques to separate the fragmentation pattern of a single component from that of others in a mixture. [2,3] In practice, the coupling of separation techniques to mass spectrometry is often combined with advanced MS techniques to achieve the desired level of accuracy and reliability of analytical information. [1,7,24-27] This chapter is about extending the range of samples that can be analyzed by mass spectrometry and about increasing the specificity of analytical information thereof. It briefly explains the basic concepts and methodologies such as handling of chromatograms, quantitation, as well as GC and LC interfaces." @default.
• W2487619324 created "2016-08-23" @default.
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• W2487619324 date "2004-01-01" @default.
• W2487619324 modified "2023-09-27" @default.
• W2487619324 title "12 Hyphenated Methods" @default.
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