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• W2488337518 abstract "The valence distribution and local structure of Bi1–xPbxNiO3 (x ≤ 0.25) were investigated by comprehensive studies of Rietveld analysis of synchrotron X-ray diffraction (SXRD) data, X-ray absorption spectroscopy (XAS), hard X-ray photoemission spectroscopy (HAXPES), and pair distribution function (PDF) analysis of synchrotron X-ray total scattering data. Disproportionation of Bi ions into Bi3+ and Bi5+ was observed for all the samples, but it was a long-ranged one with distinct crystallographic sites in the P1 triclinic structure for x ≤ 0.15, while the ordering was short-ranged for x = 0.20 and 0.25. An intermetallic charge transfer between Bi5+ and Ni2+, leading to large volume shrinkage, was observed for all the samples upon heating at ∼500 K." @default.
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• W2488337518 date "2016-08-16" @default.
• W2488337518 modified "2023-10-09" @default.
• W2488337518 title "Glassy Distribution of Bi³⁺/Bi⁵⁺ in Bi_1–<i>x</i>Pb_<i>x</i>NiO₃ and Negative Thermal Expansion Induced by Intermetallic Charge Transfer" @default.
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• W2488337518 doi "https://doi.org/10.1021/acs.chemmater.6b01160" @default.
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