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• W2489099586 endingPage "296" @default.
• W2489099586 startingPage "283" @default.
• W2489099586 abstract "Development of successful direct fluorination technology has passed through three distinct eras since 1963. The first era, called the inception, comprises the years from 1964 through 1970, and was a period in which many novel organic and inorganic classes of fluorine compounds were prepared. However, the reactions proceeded on a long time scale (up to 7 days) and gave only two to five grams of product per run. As this era closed, it was proved that finely powdered hydrocarbon solids could be converted to fluorocarbon analogs using controlled elemental fluorine as a reagent. Then came the interim period in which great advances in capabilities and yields were made. It covered the years 1970 through 1992, and was an era when direct fluorination was done in ways that had much wider applications and capabilities. Reactions were performed using a number of different reactor styles and techniques. This was the era of the disk reactor, and amelioration of reactions with many new ether and polyether structures by scavenging HF with potassium fluoride or sodium fluoride to preserve these structures. In this era, product yields normally fell in the 70–90% range, with product quantities per run ranging from five to forty grams. The third era––Renaissance (1992 to the present day)––saw the range of fluorinated inorganic, organometallic, and organic compounds. Product yields mostly exceeded 98%." @default.
• W2489099586 created "2016-08-23" @default.
• W2489099586 creator A5004877031 @default.
• W2489099586 date "2000-01-01" @default.
• W2489099586 modified "2023-10-14" @default.
• W2489099586 title "The discovery of successful direct fluorination syntheses" @default.
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• W2489099586 doi "https://doi.org/10.1016/b978-008043405-6/50030-x" @default.

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