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• W2489448536 abstract "Temperature modulated thermophysical measurements can deliver valuable insights into the phase transformation behavior of many different materials. While especially for non-metallic systems at low temperatures numerous powerful methods exist, no high-temperature device suitable for modulated measurements of bulk metallic alloy samples is available for routine use. In this work a dilatometer for temperature modulated isothermal and non-isothermal measurements in the temperature range from room temperature to 1300 K is presented. The length measuring system is based on a two-beam Michelson laser interferometer with an incremental resolution of 20 pm. The non-contact measurement principle allows for resolving sinusoidal length change signals with amplitudes in the sub-500 nm range and physically decouples the length measuring system from the temperature modulation and heating control. To demonstrate the low-amplitude capabilities, results for the thermal expansion of nickel for two different modulation frequencies are presented. These results prove that the novel method can be used to routinely resolve length-change signals of metallic samples with temperature amplitudes well below 1 K. This high resolution in combination with the non-contact measurement principle significantly extends the application range of modulated dilatometry towards high-stability phase transformation measurements on complex alloys." @default.
• W2489448536 created "2016-08-23" @default.
• W2489448536 creator A5018023553 @default.
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• W2489448536 date "2016-07-01" @default.
• W2489448536 modified "2023-09-27" @default.
• W2489448536 title "A high-stability non-contact dilatometer for low-amplitude temperature-modulated measurements" @default.
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• W2489448536 doi "https://doi.org/10.1063/1.4959200" @default.
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