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• W2489693237 abstract "Oxidation of N,N-bis(diphenylphosphanyl)naphthalen-1-amine (1) with elemental sulfur or gray selenium (1:1 molar ratio) gave the corresponding monosulfide and monoselenide bis(phosphanyl)amine ligands C10H7-1-N(P(E)Ph2)(PPh2) [E = S (2), Se (3)], respectively. Reactions of 2 and 3 with MCl2(cod) (M = Pd, Pt) afforded [MCl2{2-κ2P,S}] [M = Pd(4), Pt(5)] and [MCl2{3-κ2P,Se}] [M = Pd(6), Pt(7)], respectively. In contrast, reactions of the same ligands with NiCl2(PPh3)2 resulted in deselenization and desulfurization, producing complex 8 with the formula [NiCl2{1-κ2P,P}]. Ligands 2 and 3, as well as their complexes 4–7 and 8 were identified and characterized by multinuclear NMR (1H, 13C, 31P, and 77Se NMR) spectroscopy, elemental analysis, and IR spectroscopy. Additionally, the molecular structure of 8 was obtained." @default.
• W2489693237 created "2016-08-23" @default.
• W2489693237 creator A5057933036 @default.
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• W2489693237 date "2016-07-26" @default.
• W2489693237 modified "2023-09-27" @default.
• W2489693237 title "Synthesis and Spectroscopic Properties of PdIIand PtIIComplexes with Monosulfide and Monoselenide Bis(phosphanyl)amine Ligands" @default.
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• W2489693237 doi "https://doi.org/10.1002/zaac.201600191" @default.
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