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- W2490014792 abstract "Synthesis of a series of new 1, 3, 2� dioxaphosphin ane derivatives (3aj) was accomplished. The key step in the synthesis of 3aj involves the cyclization reaction of tris (hydroxy methyl) nitromethane (1) with P(X)Cl3 (X=S,O) in presence of TEA in THF at 40�45 °C to afford the phosphoryl mono chloride intermediate (2). The intermediate (2) when treated with different substituted aromatic amines and with a few substituted phenols in situ in the presence of TEA at 0�15 °C afforded 3aj. T he structures of 3aj were established by IR, NMR (1H, 13 C and 31 P) and Mass spectral data and elemental" @default.
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- W2490014792 date "2012-01-01" @default.
- W2490014792 modified "2023-09-26" @default.
- W2490014792 title "SYNTHESIS, SPECTRAL CHARACTERIZATION AND BIOLOGICAL ACTIVITY OF 1,3,2-DIOXAPHOSPHINANE DERIVATIVES" @default.
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