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- W2490265012 abstract "Single crystal of rare-earth polyphosphate Tm(PO 3 ) 3 has been grown under high temperature molten-salt method and structurally characterized by single crystal X-ray diffraction analysis. Using the four-dimensional superspace formalism for aperiodic structures, we performed the crystal structure refinement of Tm(PO 3 ) 3 as (3+1)-dimensional incommensurately modulated structure with monoclinic superspace group C 2/ c (0, 0.358, 0) s 0 and a = 14.0620 (12) A, b = 6.6612 (6) A, c = 10.0191 (9) A, β = 127.6043 (9) 0 , V = 743.51 (11) A 3 , Z = 4, M r = 405.8, D c = 3.626 g/cm 3 , F (000) = 744, μ (moKa) = 12.60 mm -1 , R = 0.048 and ωR = 0.050. The structure features infinite chains of corner-sharing PO 4 tetrahedra which are affected by positional modulation running along the b -axis. The final structure model was reasonable and did not show any unusual features." @default.
- W2490265012 created "2016-08-23" @default.
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- W2490265012 date "2016-06-01" @default.
- W2490265012 modified "2023-09-28" @default.
- W2490265012 title "FOUR-DIMENSIONAL INCOMMENSURATELY MODULATED STRUCTURE OF THULIUM POLYPHOSPHATE" @default.
- W2490265012 doi "https://doi.org/10.4067/s0717-97072016000200031" @default.
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