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- W2495498123 abstract "High temperature magic-angle-spinning (MAS) 1H NMR was used to identify organic components on the surface of functionalized silica nanoparticles. The high temperature data acquisition, by preferential narrowing of resonances, enabled differentiation between species that were adsorbed or weakly bound versus those that were covalently bound to the surface. MAS NMR of a sample as a slurry with appropriate solvent provided information similar to that obtained at higher temperatures. With increasing temperature, gradual separation and up-field shift of silanol proton and water resonances at different rates was observed, possibly a result of diminished hydrogen bonding at increasingly higher temperatures." @default.
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- W2495498123 date "2011-01-01" @default.
- W2495498123 modified "2023-09-25" @default.
- W2495498123 title "Proton MAS NMR Analysis of Phenyl Silane Functionalized Silica Nanoparticles" @default.
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- W2495498123 doi "https://doi.org/10.1021/bk-2011-1077.ch030" @default.
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