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• W2497284368 abstract "Five azo-functionalized coordination polymers (CPs), namely, [Zn(azbpy)(NO2-bdc)·H2O]n (1), [Zn(azbpy)(NO2-bdc)]n·3H2O (2), {[Cd(azbpy)(NO2-bdc)·H2O]·2H2O}n (3), {[Mn(azbpy)2(NO2-bdc)]2}n (4), and {[Co(azbpy)(NO2-bdc)(H2O)2][Co(azbpy)0.5(NO2-bdc)(H2O)3]}n (5) have been synthesized using different transition metal salts with 5-nitro-1,3-benzenedicarboxylate (NO2-bdc2–) and 4,4′-azobispyridine (azbpy) ligand using a slow diffusion technique at room temperature. The complexes 1–5 were characterized by single crystal X-ray diffraction analysis, elemental analysis, infrared spectroscopy (IR), powder X-ray diffraction (PXRD), and thermogravimetric analysis (TGA). In the solid state, compound 1 shows a wavy one-dimensional (1D) ladder; constructed through the N,N′-donor azbpy and NO2-bdc2– ligands with the metal centers, whereas compound 2 exhibits a bilayer two-dimensional (2D) sheet containing a wavy 1D ladder of metal-carboxylate, and compound 3 shows a stairlike wavy 2D sheet. Compound 4 exhibits a novel 2-fold interdigitated 2D sheet of two similar layers containing pendent azbpy ligands, whereas compound 5 displays a polythreaded 2D structure with an intercalated 1D chain into the pore. The solid state luminescence properties of 1–3 along with free N,N′-donor azbpy ligand have been performed at room temperature, where all the complexes 1–3 show azbpy ligand based luminescence property. The gas and solvent vapor adsorption study have been performed for compounds 2–4, and the dehydrated frameworks of compounds 2–4 exhibit selective CO2 adsorption at 195 K over N2 (at both 77 and 195 K) due to the strong interactions between polar pore walls of dehydrated frameworks with the CO2 molecule having quadruple moment." @default.
• W2497284368 created "2016-08-23" @default.
• W2497284368 creator A5032343826 @default.
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• W2497284368 creator A5078661934 @default.
• W2497284368 date "2016-08-11" @default.
• W2497284368 modified "2023-10-17" @default.
• W2497284368 title "Azo Functionalized 5-Nitro-1,3-benzenedicarboxylate Based Coordination Polymers with Different Dimensionality and Functionality" @default.
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• W2497284368 doi "https://doi.org/10.1021/acs.cgd.6b00946" @default.
• W2497284368 hasPublicationYear "2016" @default.
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