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• W2497620363 startingPage "946" @default.
• W2497620363 abstract "The synthesis of polyethylene-graft-polystyrene copolymers by a multistep grafting from approach is described. In the first step, a bromo-functional polyethylene (PE-Br) was synthesized via ring-opening metathesis polymerization (ROMP) of cis-cyclooctene (COE) and quantitative hydrobromination. Subsequent irradiation of PE-Br under visible light in the presence of dimanganese decacarbonyl (Mn2(CO)10) and 2,2,6,6-tetramethylpiperidine-1-oxyl (TEMPO) resulted in the formation of TEMPO-substituted polyethylene (PE-TEMPO). Polystyrene (PS) chains were then grown via nitroxide mediated radical polymerization (NMRP) from the PE-TEMPO precursor to give desired PE-g-PS copolymers in a controlled manner. The intermediates at each step and final graft copolymers were characterized by 1H NMR, FT-IR, GPC, and DSC analyses." @default.
• W2497620363 created "2016-08-23" @default.
• W2497620363 creator A5010588948 @default.
• W2497620363 creator A5016791337 @default.
• W2497620363 creator A5018094815 @default.
• W2497620363 creator A5060179873 @default.
• W2497620363 date "2016-07-25" @default.
• W2497620363 modified "2023-10-17" @default.
• W2497620363 title "Polyethylene-<i>g</i>-Polystyrene Copolymers by Combination of ROMP, Mn₂(CO)₁₀-Assisted TEMPO Substitution and NMRP" @default.
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• W2497620363 doi "https://doi.org/10.1021/acsmacrolett.6b00460" @default.
• W2497620363 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/35607209" @default.
• W2497620363 hasPublicationYear "2016" @default.
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