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- W250205700 abstract "The crystal structure of the title compound {[Mn(phen)2(OAc)(H2O)]ClO4}2.H2O(phen=1,10-phenanthroline)has been synthesized and determined by X-ray diffraction.The crystal is of triclinic,space group P1 with a=12.7955(4),b=15.0544(4),c=16.2183(4)A,a=64.479(1)β=67.526(1)，γ=83.582(1)°,C52H40Cl2Mn2N8O15,Mr=1197.70,V=2600.1(1)A^3,Dc=1.530g/cm^3,F(000)=1224,μ-0.666cm^-1 and Z=2.The final refinement gave R=0.0691 and WR=0.1821 for 6131 observed reflections with I>2σ(I),The cell of the complex contains two uniform mono-manganese molecules {[Mn(phen)2(OAc)(H2O)]ClO4 and a solvate water molecule.Four nitrogen atoms from two chelating phenanthroline ligands and one oxygen atom from acetate ligate to the Mn^11 ion,forming a distorted octahedral geometry together with one coordinated water molecule,One ClO4^- anion and one water molecule exist outside the cation {[Mn(phen)2(OAc)(H2O)]^+ as a counter ion and solvate molecule,respectively." @default.
- W250205700 created "2016-06-24" @default.
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- W250205700 date "2003-01-01" @default.
- W250205700 modified "2023-09-24" @default.
- W250205700 title "Synthesis and Strutural Characterization of {[Mn（phen）2（OAc）（H2O）]ClO4}2.H2O" @default.
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