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- W2502585621 abstract "Fe3O4@SiO2 with 3D core–shell nanoparticles were used to immobilize Fe(acac)3/2,6-bis(1-(2-isopropylanilinoethyl)) in order to polymerize ethylene in a confined geometry. Structural and morphological evolution of nascent polyethylene is particularly studied. The dependence of molecular weight, molecular weight distribution, condensed structure, and dispersion of nanoparticles on the polymerization time are investigated quantitatively. Both the molecular weight and the molecular weight distribution of synthesized polymers gradually increase as the polymerization proceeds. It is found that the nascent polymer contains a monoclinic phase and a weakly entangled state due to the confined polymerization environment and the low temperature of polymerization. This is the first time that the monoclinic phase is observed in the nascent polyethylene with Mw less than 1 × 105 g/mol. Magnetic property of the polyethylene is presented, as is expected. Finally, fragmentation of Fe3O4@SiO2 nanoparticles during the polyme..." @default.
- W2502585621 created "2016-08-23" @default.
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- W2502585621 date "2016-08-04" @default.
- W2502585621 modified "2023-10-16" @default.
- W2502585621 title "Structural and Morphological Evolution of Nascent Polyethylene during Ethylene <i>in Situ</i> Polymerization within Fe<sub>3</sub>O<sub>4</sub>@SiO<sub>2</sub> Nanoparticles" @default.
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- W2502585621 doi "https://doi.org/10.1021/acs.iecr.6b01312" @default.
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