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• W2503693213 abstract "The Met-enkephalin, Tyr-Gly-Gly-Phe-Met, was synthesized by the solution-phase synthesis (SPS) methodology employing -OBzl group as carboxyls' protection, while the t-Boc groups were employed for the N-terminal α-amines' protection for the majority of the amino acids of the pentapeptide sequence. The l-methionine (l-Met) amino acid was used as PTSA.Met-OBzl obtained from the simultaneous protection of the α-amino, and carboxyl group with para-toluene sulfonic acid (PTSA) and as-OBzl ester, respectively in a C-terminal start of the 2 + 2 + 1 fragments condensation convergent synthetic approach. The protection strategy provided a short, single-step, simultaneous, orthogonal, nearly quantitative, robust, and stable process to carry through the protected l-methionine and l-phenylalanine coupling without any structural deformities during coupling and workups. The structurally confirmed final pentapeptide product was feasibly obtained in good yields through the current approach." @default.
• W2503693213 created "2016-08-23" @default.
• W2503693213 creator A5010591387 @default.
• W2503693213 date "2016-08-20" @default.
• W2503693213 modified "2023-09-27" @default.
• W2503693213 title "Synthesis of Met-enkephalin by solution-phase peptide synthesis methodology utilizingpara-toluene sulfonic acid as N-terminal masking ofl-methionine amino acid" @default.
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• W2503693213 doi "https://doi.org/10.1111/cbdd.12821" @default.
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