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- W2508308664 abstract "Abstract Technical chlordane is extracted in acetone, diluted with hexane, and determined via capillary gas chromatography with electron capture detection. Quantitation is based on the sum of areas or heights of 6 well resolved major peaks. The method was tested for precision, linearity, recovery, and applicability to aqueous dilutions of emulsifiable concentrate formulations. Comparison of quadruplicate analysis of 5 formulations by this method with the AOAC official titrimetric method gave average relative standard deviations of 1.4 and 0.9 %, respectively. Results were comparable for the 72% formulations, but were lower using this method for the 45% samples. Linearity and recovery were excellent (regression coefficient = 0.9996, recovery = 100.7%). Application of this method to aqueous dilutions was simple and resulted in an average recovery of 97%. The method is faster, safer, and more specific than the AOAC titrimetric method." @default.
- W2508308664 created "2016-09-16" @default.
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- W2508308664 date "1985-03-01" @default.
- W2508308664 modified "2023-09-26" @default.
- W2508308664 title "Capillary Gas Chromatographic Determination of Technical Chlordane in Emulsifiable Concentrates and Aqueous Dilutions" @default.
- W2508308664 doi "https://doi.org/10.1093/jaoac/68.2.175" @default.
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