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- W2509482173 abstract "Abstract The synergetic effects SiC particles and short carbon fibers (C sf ) as well as hot pressing parameters (sintering temperature, dwell time and applied pressure) on the grain growth of ZrB 2 -based composites were investigated. Taguchi methodology was employed for the design of experiments to study the microstructure and grain growth of ZrB 2 –SiC–C sf ceramic composites. Three hot pressing parameters and SiC/C sf ratio were selected as the scrutinized variables. The sintering temperature and SiC/C sf ratio were identified by ANOVA as the most effective variables on the gain growth of ZrB 2 -based samples. Removal of oxide impurities from the surface of starting particles by the reactant C sf , not only hindered the extraordinary grain growth of ZrB 2 matrix, but also improved the sinterability of the ceramics. A fully dense ceramic with an average grain size of 8.3 µm was obtained by hot pressing at 1850 °C for 30 min under 16 MPa through adding 20 vol% SiC and 10 vol% C sf to the ZrB 2 matrix. SEM observations and EDS analysis verified the in-situ formation of ZrC which can restrain the growth of ZrB 2 particles, similar to the role of SiC, by the pinning of grain boundaries as another stationary secondary phase." @default.
- W2509482173 created "2016-09-16" @default.
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- W2509482173 date "2016-12-01" @default.
- W2509482173 modified "2023-09-24" @default.
- W2509482173 title "Synergetic effects of SiC and Csf in ZrB2-based ceramic composites. Part II: Grain growth" @default.
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- W2509482173 doi "https://doi.org/10.1016/j.ceramint.2016.08.205" @default.
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