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• W2511201702 abstract "A real-time study of the growth of two-dimensional nanocrystal superlattices with square periodicity shows the formation mechanism leading to the oriented attachment of the nanocrystals. Oriented attachment of PbSe nanocubes can result in the formation of two-dimensional (2D) superstructures with long-range nanoscale and atomic order1,2. This questions the applicability of classic models in which the superlattice grows by first forming a nucleus, followed by sequential irreversible attachment of nanocrystals3,4, as one misaligned attachment would disrupt the 2D order beyond repair. Here, we demonstrate the formation mechanism of 2D PbSe superstructures with square geometry by using in situ grazing-incidence X-ray scattering (small angle and wide angle), ex situ electron microscopy, and Monte Carlo simulations. We observed nanocrystal adsorption at the liquid/gas interface, followed by the formation of a hexagonal nanocrystal monolayer. The hexagonal geometry transforms gradually through a pseudo-hexagonal phase into a phase with square order, driven by attractive interactions between the {100} planes perpendicular to the liquid substrate, which maximize facet-to-facet overlap. The nanocrystals then attach atomically via a necking process, resulting in 2D square superlattices." @default.
• W2511201702 created "2016-09-16" @default.
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• W2511201702 date "2016-09-05" @default.
• W2511201702 modified "2023-10-01" @default.
• W2511201702 title "In situ study of the formation mechanism of two-dimensional superlattices from PbSe nanocrystals" @default.
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• W2511201702 doi "https://doi.org/10.1038/nmat4746" @default.
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