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- W2511662612 abstract "Abstract Trivanadium-substituted heteropolytungstates, α- and β-K6H-[GeW9V3Q40]∗ xH2O (α- and β-GeW9V3), have been synthesized from their lacunary precursors, α- and β- [GeW9O34]10, and characterized by elemental analysis, cyclic voltammograms and 51V and 183NMR spectra. 183w NMR spectra of the title anions consist of tulo lines (intensity ratio 2 : 1) as expected for the C3V structure of trisubstituted α- and β-Keggin anions. The 2Jw.o.w couplings of the title anions exhibit sharper lines (19.35 and 16.73 Hz. respectively), confirming that the title complexes contain substituted vanadium in adjacent comer-shared octahedra of α- and β-Keggin structures, respectively. The solution ESR spectra of the one-electron-reduced anions consist of more than 40 equally spaced lines, showing that the three VO6 octahedra in both α- and β-fom are comer-shared and one of the bridging oxygen atams is protonated at pH 4.7." @default.
- W2511662612 created "2016-09-16" @default.
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- W2511662612 date "1998-07-01" @default.
- W2511662612 modified "2023-09-26" @default.
- W2511662612 title "Synthesis and<sup>183</sup>W and<sup>51</sup>V Nmr Characterization of α- and β-K<sub>6</sub>H[Gew<sub>9</sub>V<sub>3</sub>O<sub>40</sub>].Xh<sub>2</sub>O and Esr Spectra of Mixed-Valence Vanadium Polyanions" @default.
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- W2511662612 doi "https://doi.org/10.1080/00945719809351674" @default.
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