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• W2513524995 abstract "Abstract Physical vapour deposition of Phosphate-based glasses enables their application onto load bearing implant surfaces for their potential to enhance osseointegration by leaching therapeutic ions at the bone/implant interface. Structural understanding with respect to processing parameters will prove useful in the on-going production of multi-functional coatings for antibacterial ion release and osseous tissue integration. This study highlights significant differences in short-range structural variation between vapour condensed and conventional melt-quenched phosphate glasses, via 31 P MAS-NMR, XPS, FTIR and DTA. Three coating compositions containing P 2 O 5 - 32.5, 34 and 37 mol% showed greater bulk network polymerisation based on the presence of (23% to 45% Q 2 species) versus (9% to 32% Q 2 species) in melt-quenched glasses as determined by NMR. The proportion of P-O-P bridging oxygens as suggested by XPS on the surface of coatings remained consistent at (34% to 35%) forming (PO 3 ) − metaphosphates (Q 2 ), whilst P‐O‐P bonding in melt-quenched glasses increased from (12% to 18%) and were found to form (PO 4 ) 3 − orthophosphates (Q 0 ) and (P 2 O 7 ) 4 − pyrophosphates (Q 1 ). AFM analysis of the coating surfaces showed nano-topographical changes due to etch pitting, which led to Ra increases from 19 nm to 167 nm, which correlated to an increased deposition rate and therefore bombardment energy." @default.
• W2513524995 created "2016-09-16" @default.
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• W2513524995 date "2016-12-01" @default.
• W2513524995 modified "2023-09-24" @default.
• W2513524995 title "Insights into structural characterisation and thermal properties of compositionally equivalent vapour-condensed and melt-quenched glasses" @default.
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• W2513524995 doi "https://doi.org/10.1016/j.matdes.2016.08.063" @default.
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