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- W2514651648 abstract "The title compound, [Rh(C 8 H 12 )(C 18 H 16 NP)]BF 4 has been prepared as a precatalyst for applications in rhodium-catalysed additions of carbocyclic acids to terminal alkynes leading to anti -Markovnikov Z -enol esters. Here the triclinic pseudopolymorph of the title compound is presented. In contrast to the earlier reported pseudopolymorph (orthorhombic space group) [Wei et al. (2013). Chem. Eur. J. 19 , 12067–12076], the triclinic polymorph contains half a molecule of dichloromethane as solvent in the asymmetric unit. The rhodium(I) atom exhibits a square-planar coordination. The estimated diffraction contribution of the disordered solvent (a half molecule of dichloroethane per asymmetric unit) was subtracted from the observed diffraction data using the SQUEEZE [Spek (2015). Acta Cryst. C 71 , 9–16] routine in PLATON . The given chemical formula and other crystal data do not take the solvent into account." @default.
- W2514651648 created "2016-09-16" @default.
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- W2514651648 date "2016-08-26" @default.
- W2514651648 modified "2023-09-27" @default.
- W2514651648 title "(η<sup>2</sup>,η<sup>2</sup>-Cycloocta-1,5-diene)[2-(diphenylphosphanylmethyl)pyridine-κ<sup>2</sup><i>N</i>,<i>P</i>]rhodium(I) tetrafluoridoborate 1,2-dichloroethane monosolvate" @default.
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- W2514651648 doi "https://doi.org/10.1107/s2414314616013183" @default.
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