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• W2515565063 abstract "Abstract In the present study, the cations Co 2+ /Ni 2+ and Al 3+ distribution in nanocrystalline (Co, Ni)Al 2 O 4 spinel have been investigated using X-ray and transmission electron microscopy. The nanocrystalline (Co, Ni)Al 2 O 4 spinel has been synthesized using mechanically activated Al 70 Co 15 Ni 15 quasicrystalline precursor through annealing at 600 °C in controlled oxygen atmosphere. The mechanical activation of single phasic decagonal Al 70 Co 15 Ni 15 quasicrystal was carried out in a high energy attritor ball mill for 40 h with 40:1 ball to powder ratio using toluene as a process control agent. The high resolution x-ray diffraction data has been refined by the Rietveld method using JANA2006 and subsequently, the corresponding structure has been constructed using Diamond4.0. The structure was also confirmed by analysis of transmission electron microscopy linearized diffraction pattern profile of d -values and corresponding plane. These analyses indicate that the cations Co 2+ and Ni 2+ distributed in the tetrahedral coordinated sites are the dominant species in the normal spinel phase." @default.
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• W2515565063 date "2016-12-01" @default.
• W2515565063 modified "2023-09-27" @default.
• W2515565063 title "Cation distribution in nanocrystalline (Co, Ni)Al2O4 Spinel" @default.
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• W2515565063 doi "https://doi.org/10.1016/j.ceramint.2016.08.193" @default.
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