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- W2515665612 abstract "In this report, a technique of single-crystal X-ray diffraction measurements under high pressures, using a diamond-anvil-cell with helium gas as an inert and hydrostatic pressure-transmitting medium, is introduced. The technique has been applied to three-dimensional halogen-bridged mixed-valence gold complexes, Cs2AuIAuIIIX6 (X=Cl, I) to investigate the mixed-valence state and the crystal structure under high pressures up to 18 GPa and 7. 5 GPa, respectively. The pressure dependences of the unit cell parameters indicate that structural phase transitions occur from tetragonal to cubic at 12. 5 GPa for the Cl-bridged complex, and from tetragonal to monoclinic at 6. 0 GPa for the I-bridged complex. The Cl-bridged complex in the higher pressure phase has a space group, Pm3m and the cubic Perovskite-type structure." @default.
- W2515665612 created "2016-09-16" @default.
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- W2515665612 date "1998-01-01" @default.
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- W2515665612 title "Single Crystal X-Ray Structure Analysis under High Pressure Using He Gas as a Pressure Transmitting Medium. Crystal Structure of Mixed-Valence Complexes Cs2AuIAuIIIX6." @default.
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- W2515665612 doi "https://doi.org/10.4131/jshpreview.8.280" @default.
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