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• W2516172296 abstract "The hydrates [Na2(H2O)3(Htba)2] (1) and [Na2(H2O)4(Htba)2] (2), where H2tba is 2-thiobarbituric acid, were obtained under different thermal conditions from aqueous solutions and were structurally characterized. The molecular and supramolecular structures were compared to the known structure of [Na2(H2O)5(Htba)2] (3). In polymeric 1–3, the Htba− ions are linked to Na+ through O and S forming octahedra. The decrease of the number of coordination water molecules led to an increase of the total number of bridge ligands (μ2-H2O, Htba−) and a change of the Htba− coordination. These factors induced higher distortion of the octahedra. It was assumed that hydrates, with a different number of coordinated water molecules, are more probable when the central metal has weaker bonds with O water molecules and with other ligands. The net topologies of 1–3 were compared. Thermal decomposition and IR spectra were analyzed for 1 and 2." @default.
• W2516172296 created "2016-09-16" @default.
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• W2516172296 date "2016-09-06" @default.
• W2516172296 modified "2023-10-14" @default.
• W2516172296 title "Hydrates [Na₂(H₂O)_x](2-thiobarbiturate)₂ (<i>x</i> = 3, 4, 5): crystal structure, spectroscopic and thermal properties" @default.
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• W2516172296 doi "https://doi.org/10.1080/00958972.2016.1228914" @default.
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