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• W2516202504 endingPage "2746" @default.
• W2516202504 startingPage "2738" @default.
• W2516202504 abstract "The syntheses of the intramolecularly coordinated organotin compounds {Me2N(CH2)3}Ph(X)SnCH2SnPh2X (3, X = I; 4, X = F) and {Me2N(CH2)3}Ph(F)Sn(CH2)3SnPh2F (7) are reported. The compounds have been characterized by elemental analysis, electrospray mass spectrometry, 1H,1H DOSY (4), 13C, 19F, and 119Sn NMR spectroscopy, and single-crystal X-ray diffraction analysis. In the solid state, compound 4 is a head-to-tail dimer as a result of unsymmetrical Sn–F–Sn bridges, whereas compound 7 is a monomer with F→Sn intramolecular coordination, giving a six-membered ring. In solution, both 4 and 7 are monomeric. The reactions of both 4 and 7 with fluoride anion in CD2Cl2 have been investigated by variable-temperature 19F and 119Sn NMR spectroscopy." @default.
• W2516202504 created "2016-09-16" @default.
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• W2516202504 date "2016-08-08" @default.
• W2516202504 modified "2023-10-01" @default.
• W2516202504 title "Unsymmetrical Bicentric Organotin Lewis Acids {Me₂N(CH₂)₃}Ph(X)Sn(CH₂)_<i>n</i>SnPh₂X (X = F, I; <i>n</i> = 1, 3): Syntheses and Structures" @default.
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• W2516202504 doi "https://doi.org/10.1021/acs.organomet.6b00500" @default.
• W2516202504 hasPublicationYear "2016" @default.
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