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- W2516511105 abstract "The synthesis of a series of recyclable iron-based extractants for the extraction and recovery of ReO{sub 4}{sup -} and TcO{sub 4}{sup -} from aqueous media will be described. The extractants are [Fe(Cp{prime}){sub 2}{sup +}][NO{sub 3}{sup -}] and [Fe(Tp{prime}){sub 2}{sup +}][NO{sub 3}{sup -}], where Cp{prime} and Tp{prime} are substituted cyclopentadienyl and tris(pyrazolylborate), respectively. The solubility of the extractants in organic solvents and aqueous solution, the stability of the extractants as a function of pH, and the ReO{sub 4}{sup -}/TcO{sub 4}{sup -} extraction efficacy vary as a function of alkyl substituent groups on the Cp{prime} and Tp{prime} ligands. The perrhenate or pertechnetate ions were recovered from the organic phases as M(ReO{sub 4}){sub n} or M(TcO{sub 4}){sub n} salts by treatment with a variety of metal powders, M, which also allowed for the recovery and reuse of Fe(Cp{prime}){sub 2} and Fe(Tp{prime}){sub 2}." @default.
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- W2516511105 date "1996-10-01" @default.
- W2516511105 modified "2023-09-26" @default.
- W2516511105 title "Extraction and recovery of ReO{sub 4}-using Fe(II)/Fe(III) complexes" @default.
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