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• W2517299536 startingPage "12041" @default.
• W2517299536 abstract "Poly(lactic acid) (PLA) is a biodegradable polymer prepared by the catalyzed ring opening polymerization of lactide. An ideal catalyst should enable a sequential polymerization of the lactide enantiomers to afford stereoblock copolymers with predetermined number and lengths of blocks. We describe a magnesium based catalyst that combines very high activity with a true-living nature, which gives access to PLA materials of unprecedented microstructures. Full consumption of thousands of equivalents of L-LA within minutes gave PLLA of expected molecular weights and narrow molecular weight distributions. Precise PLLA-b-PDLA diblock copolymers having block lengths of up to 500 repeat units were readily prepared within 30 min, and their thermal characterization revealed a stereocomplex phase only with very high melting transitions and melting enthalpies. The one pot sequential polymerization was extended up to precise hexablocks having dialed-in block lengths." @default.
• W2517299536 created "2016-09-16" @default.
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• W2517299536 date "2016-09-12" @default.
• W2517299536 modified "2023-10-17" @default.
• W2517299536 title "Tailor-Made Stereoblock Copolymers of Poly(lactic acid) by a Truly Living Polymerization Catalyst" @default.
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• W2517299536 doi "https://doi.org/10.1021/jacs.6b07287" @default.
• W2517299536 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/27602949" @default.
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