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• W2517931900 abstract "A general method for the N-arylation of amino acid esters with aryl triflates is described. Both α- and β-amino acid esters, including methyl, tert-butyl, and benzyl esters, are viable substrates. Reaction optimization was carried out by design of experiment (DOE) analysis using JMP software. The mild reaction conditions, which use t-BuBrettPhos Pd G3 or G4 precatalyst, result in minimal racemization of the amino acid ester. This method is the first synthetic application of the t-BuBrettPhos Pd G4 precatalyst. Mechanistic studies show that the observed erosion in enantiomeric excess is due to racemization of the amino acid ester starting material and not of the product." @default.
• W2517931900 created "2016-09-16" @default.
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• W2517931900 date "2016-08-08" @default.
• W2517931900 modified "2023-09-29" @default.
• W2517931900 title "Development of a Method for the N-Arylation of Amino Acid Esters with Aryl Triflates" @default.
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• W2517931900 doi "https://doi.org/10.1021/acs.orglett.6b02082" @default.
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