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- W2518506649 abstract "The title isotypic complexes, bis[μ-5,6-bis(pyridin-2-yl)pyrazine-2,3-dicarboxylato]-κ 4 N 1 , O 2 , N 6 : O 3 ;κ 4 O 3 : N 1 , O 2 , N 6 -bis[diaquamanganese(II)] tetrahydrate, [Mn 2 (C 16 H 8 N 4 O 4 ) 2 (H 2 O) 4 ]·4H 2 O, (I), and bis[μ-5,6-bis(pyridin-2-yl)pyrazine-2,3-dicarboxylato]-κ 4 N 1 , O 2 , N 6 : O 3 ;κ 4 O 3 : N 1 , O 2 , N 6 -bis[diaquairon(II)] tetrahydrate, [Fe 2 (C 16 H 8 N 4 O 4 ) 2 (H 2 O) 4 ]·4H 2 O, (II), are, respectively, the manganese(II) and iron(II) complexes of the ligand 5,6-bis(pyridin-2-yl)-pyrazine-2,3-dicarboxylic acid. The complete molecule of each complex is generated by inversion symmetry. Each metal ion is coordinated by a pyrazine N atom, a pyridine N atom, two carboxylate O atoms, one of which is bridging, and two water O atoms. The metal atoms have M N 2 O 4 coordination geometries and the complexes have a cage-like structure. In the crystals of both compounds, the complexes are linked by O—H...O and O—H...N hydrogen bonds involving the coordinating water molecules, forming chains along [100]. These chains are linked by O—H...O hydrogen bonds involving the non-coordinating water molecules, forming layers parallel to (011). The layers are linked by pairs of C—H...O hydrogen bonds and offset π–π interactions, so forming a hydrogen-bonded three-dimensional framework." @default.
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- W2518506649 date "2016-09-09" @default.
- W2518506649 modified "2023-10-18" @default.
- W2518506649 title "Isotypic MnIIand FeIIbinuclear complexes of the ligand 5,6-bis(pyridin-2-yl)-pyrazine-2,3-dicarboxylic acid" @default.
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- W2518506649 doi "https://doi.org/10.1107/s2056989016014055" @default.
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