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- W2520565035 abstract "Feasibility studies on the crystallization of Zr hydroxide to ZrO{sub 2} in aqueous solutions were performed at 100{degrees}C and 25{degrees}C. The main objective of this work is to demonstrate synthesis of crystalline ZrO{sub 2} powders in an open vessel (i.e. at or below the boiling point of the aqueous solutions). Boiling treatments of Zr hydroxide suspensions were carried out at pH 9.5 and 13.9. Crystallization of amorphous Zr hydroxide to a mixture of monoclinic and cubic ZrO{sub 2} at 100{degrees}C was demonstrated at pH 13.9 within reasonable reaction time (2 hours). Even at 25{degrees}C, crystallization occurred at pH 13.9. In contrast, crystallization at pH 9.5 did not occur at 100{degrees}C. The crystallization mechanism of Zr hydroxide to ZrO{sub 2} is discussed based on the solution chemistry of Zr{sup 4+} and gel chemistry of Zr hydroxide." @default.
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- W2520565035 date "1995-12-31" @default.
- W2520565035 modified "2023-09-27" @default.
- W2520565035 title "Crystallization of Zr hydroxide to ZrO{sub 2} at/or below 100{degrees}C" @default.
- W2520565035 hasPublicationYear "1995" @default.
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