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- W2523642711 abstract "Irradiation of 4,4-dimethyl-3-[(2-cyclopentenyl)methoxy]-2-cyclohexen-1-one, prepared from 4,4-dimethyl-3-phenylthio-2-cyclohexen-1-one and (2-cyclopentenyl) methanol, gave a tetracyclic intramolecular [2+2]photocycloadduct 7. Treatment of 7 with iodotrimethylsilane followed with tributyltin hydride afforded 3,3,11-trimethylbicyclo[6.3.0]undecane-2,6-dione(12). Methylenation of 12 afforded 6-methylene-3,3,11-trimethylbicyclo[6.3.0] undecan-2-one, the known intermediate to precapnelladiene." @default.
- W2523642711 created "2016-09-30" @default.
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- W2523642711 date "2006-08-05" @default.
- W2523642711 modified "2023-09-24" @default.
- W2523642711 title "Preparation of An 8-Membered Ring via Intramolecular [2+2]Photocycloadduct: Formal Total Synthesis of (±)-Precapnelladiene" @default.
- W2523642711 hasPublicationYear "2006" @default.
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