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- W2527648731 abstract "Dissolution dynamic nuclear polarization (D-DNP) has become a method of choice to enhance signals in nuclear magnetic resonance (NMR). Recently, we have proposed to combine cross-polarization (CP) with D-DNP to provide high polarization P(13C) in short build-up times. In this paper, we show that switching microwave irradiation off for a few hundreds of milliseconds prior to CP can significantly boost the efficiency. By implementing microwave gating, 13C polarizations on sodium [1-13C]acetate as high as 64% could be achieved with a polarization build-up time constant as short as 160 s. A polarization of P(13C) = 78% could even be reached for [13C]urea." @default.
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- W2527648731 date "2016-01-01" @default.
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- W2527648731 title "Microwave-gated dynamic nuclear polarization" @default.
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- W2527648731 doi "https://doi.org/10.1039/c6cp05587g" @default.
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