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• W2528448052 abstract "Abstract An original method for the synthesis of substituted phosphines R2P(X)BuR′ (R′ = n-Hex, Bn, napht, cyclo-Hex) and R2P(X)EtR′ (R′ = 2-bycyclo[2.2.1]hept-2-yl) (R = Et, Ph, X = O, S), in 65–72% yield has been developed via the interaction between halophosphines R2PCl (R = Et, Ph) and aluminacyclopentanes, generated in situ from alkenes and Et3Al in the presence of Cp2ZrCl2. The synthesized phosphines were found to react with Mo(CO)6 giving rise to molybdenum complexes Mo(CO)5L (L = 4a; 3b; 3c). The interaction between (2-bicyclo[2.2.1]hept-2-ylethyl)diphenylphosphine and Pd(COD)Cl2 leads to compound of the type L2PdCl2. Structures of new compounds were determined using X-ray diffraction techniques and multinuclear (1H, 13C, and 31P) NMR spectroscopy." @default.
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• W2528448052 date "2016-12-01" @default.
• W2528448052 modified "2023-10-18" @default.
• W2528448052 title "Zirconium-catalyzed alkene cycloalumination for the synthesis of substituted phosphines and their transition metal (Mo, Pd) complexes" @default.
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• W2528448052 doi "https://doi.org/10.1016/j.jorganchem.2016.10.012" @default.
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