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- W2528863003 abstract "Quinoline-imine nickel (II) complexes were immobilized in fluorotetrasilicic mica interlayers by a one-pot synthesis through the reaction of a nickel ion-exchanged fluorotetrasilicic mica (Ni2+-mica) with the corresponding quinoline and aniline derivatives. After activation of the prepared precatalyst by a co-catalyst (Et3Al, iBu3Al, or Et2AlCl), it showed a high catalytic activity for the oligomerization of ethylene with the formation of oligomers having carbon numbers 4–20. The maximum activity (168 g-product g-cat−1 h−1) was obtained by the oligomerization at 40 °C and 1.0 MPa in the presence of Et3Al using the precatalyst prepared from Ni2+-mica, 2-acetylquinoline, and 2, 6-dimethylaniline. In all the oligomerization runs, a long induction period was observed, and the induction time significantly depended on the co-catalyst. This induction period might be caused by the characteristic structure of the precatalysts. The FT-IR and XRD spectra of the precatalysts indicated the formation of the intended nickel complexes in the mica interlayer." @default.
- W2528863003 created "2016-10-14" @default.
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- W2528863003 date "2016-12-01" @default.
- W2528863003 modified "2023-09-23" @default.
- W2528863003 title "Ethylene oligomerization using quinoline-imine nickel(II) complex immobilized in fluorotetrasilicic mica interlayer by one-pot preparation method" @default.
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- W2528863003 doi "https://doi.org/10.1016/j.molcata.2016.10.005" @default.
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