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• W2531054071 abstract "An analytical method has been developed for the quantitative determination of polycyclic aromatic hydrocarbons (PAHs) and their nitrated and oxygenated derivatives (nitro- and oxy-PAHs respectively) in particulate matter (PM) samples. The sample preparation procedure included only a simple and quick sonication-assisted extraction step, clean-up based on addition of water and centrifugation as well as pre-concentration under N2 stream. The determination of 16 PAHs and 4 oxy-PAHs was carried out by gas chromatography–mass spectrometry, while liquid chromatography–tandem mass spectrometry was used in the case of the 11 investigated nitro-PAHs. The optimized method was fully evaluated in terms of trueness, precision (repeatability), limit of detection (LOD), limit of quantification (LOQ), sensitivity and linearity. The LOQ values ranged at pg m−3 level for the investigated PAHs (42 pg m−3), oxy-PAHs (either 42 or 83 pg m−3) and nitro-PAHs (either 83 or 167 pg m−3) as well. The developed method was applied for the quantitative determination of PAHs, nitro- and oxy-PAHs in urban PM2.5 (particles with aerodynamic diameter smaller than 2.5 μm) samples (n = 36) collected in Budapest, Hungary. Almost 100% of the PM2.5 samples contained the investigated PAHs and oxy-PAHs in detectable and quantifiable amounts; however, the concentration of the nitro-PAHs was generally lower than the corresponding LOD/LOQ values. According to our results, during the 3-year long sampling campaign the concentration of benzo(a)pyrene never exceeded the limit value (1 ng m−3) set by the European Commission." @default.
• W2531054071 created "2016-10-21" @default.
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• W2531054071 date "2016-11-01" @default.
• W2531054071 modified "2023-10-10" @default.
• W2531054071 title "Determination of particulate phase polycyclic aromatic hydrocarbons and their nitrated and oxygenated derivatives using gas chromatography–mass spectrometry and liquid chromatography–tandem mass spectrometry" @default.
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• W2531054071 doi "https://doi.org/10.1016/j.chroma.2016.10.021" @default.
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