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• W2531875722 endingPage "1767" @default.
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• W2531875722 abstract "Simultaneous multiple data set fits of all transition peaks of 133Cs nuclei enabled us to obtain accurate cesium-133 nuclear magnetic resonance (NMR) parameters and Euler angles between the principal axis systems of the chemical shift (CS) and quadrupole coupling (Q) tensors of 133Cs nuclei in Cs2CrO4 . Although in a previous study of Cs2CrO4 by Power et al. (W. P. Power, S. Mooibroek, R. E. Wasylishen, T. S. Cameron, J. Phys. Chem. 1994, 98, 1552), one central transition was observed for cesium sites 1 and 2 in the 133Cs NMR spectra and one Euler angle between the CS tensors and Q tensors was obtained as 52° and 7° for cesium sites 1 and 2, respectively, the present single-crystal 133Cs NMR measurements found two Euler angles (10(2)°, 51.9(1)°, 0°) for site 1 and two central transition peaks for site 2. Three principal components of the CS tensor for Cs1 are oriented along the crystallographic a, b, and c axes, whereas none of the principal components of the Q tensor for Cs1 are oriented along the crystal axes. The principal component V 22 of the Q tensor for Cs1 is tilted 10° from the b axis in the bc plane, and the other two components are not located in the ac plane. Therefore, we have found that the requirement that “the quadrupole coupling tensor for a nucleus located in a mirror plane has one principal axis perpendicular to the mirror plane” cannot be applied to Cs1. On the other hand, δ11 and V 22 for Cs2 are aligned along the b axis, and the other components of the CS and Q tensors deviate at an angle of 1.4(1)° and 10.1(1)°, respectively, from the a and c axes in the ac plane. A distortion-free powder 133Cs NMR spectrum of Cs2CrO4 was measured using a solid-state spin echo technique." @default.
• W2531875722 created "2016-10-21" @default.
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• W2531875722 date "2016-10-12" @default.
• W2531875722 modified "2023-10-15" @default.
• W2531875722 title "Symmetry Breaking Nuclear Quadrupole Coupling Tensor Orientation for Cesium-133 Nuclei Located in a Mirror Plane" @default.
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• W2531875722 doi "https://doi.org/10.1002/bkcs.10965" @default.
• W2531875722 hasPublicationYear "2016" @default.
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