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- W2532332344 abstract "Abstract Florida citrus depends on a breakthrough in the fight against citrus greening disease. Of the antibiotics used to treatthis disease, penicillin G has been one of the most effective. Because orange fruit grown in the state of Florida are mainly used to produce orange juice, we have validated an ultra-HPLC tandem MS method to screen for penicillin G and its metabolites (penillic and penilloic acids) at the chemical residue level after treatment. In this method, three spike levels (0.25, 1, and 20 ng/g) were tested in triplicate. Absolute recoveries for penillic and penilloic acids were 60–75% depending on the matrix used, whereas corrected recoveries of penicillin G using an isotopically labeled internal standard were ~100%. Two product ion transitions per analyte were required for identification, which contributes to a high degree of selectivity." @default.
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- W2532332344 date "2017-01-01" @default.
- W2532332344 modified "2023-09-27" @default.
- W2532332344 title "LC-MS/MS Validation of a Residue Analysis Method for Penicillin G and Its Metabolites in Commercial Orange Juice" @default.
- W2532332344 doi "https://doi.org/10.5740/jaoacint.16-0166" @default.
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