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• W2533014749 abstract "Abstract Four aryl‐substituted tripyrrinone copper(II) complexes were synthesized and characterized as to their electrochemical and spectroelectrochemical properties. The examined compounds are represented as (YPh) 3 TPO 2 Cu, where TPO 2 is a dianion of the tripyrrinone and Y is a CH 3 O, CH 3 , H or Cl substituent on the para ‐position of each phenyl ring of the compound. The neutral compounds are ESR active and show a typical d 9 Cu(II) signal in frozen CH 2 Cl 2 solution. Each Cu(II) compound undergoes three reductions between −0.61 and −1.90 V and two oxidations between 1.00 and 1.24 V in CH 2 Cl 2 containing 0.1 mol/L tetra‐ n ‐butylammonium perchlorate. The potentials for oxidation are similar to those of copper tetraarylporphyrins but the reduction potentials are positively shifted as compared to the corresponding tetraarylporphyrins. Thus, the potential difference between the first one‐electron oxidation and first one‐electron reduction (the HOMO‐LUMO gap) of (YPh) 3 TPO 2 Cu, which ranges from 1.68 to 1.75 V, is similar to that of copper corroles (1.73–1.85 V), but smaller than the separation of 2.30–2.37 V for the copper tetraarylporphyrins under the same solution conditions." @default.
• W2533014749 created "2016-10-28" @default.
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• W2533014749 date "2016-10-01" @default.
• W2533014749 modified "2023-10-06" @default.
• W2533014749 title "Synthesis and Electrochemistry of Aryl-Substituted Tripyrrinone Copper Complexes. Comparison of Redox Properties to Structurally Related Porphyrins and Corroles" @default.
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• W2533014749 doi "https://doi.org/10.1002/cjoc.201600484" @default.
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