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- W2539929467 abstract "Abstract In this study, a reliable method based on the combination of ion molecule reaction ICP-MS and addition of a CH 4 plasma modifier technique was established for the direct determination of Se in Ca-rich groundwater samples. The 80 Se + was oxidized to 80 Se 16 O + by O 2 , and detected at m / z 96. Under the optimized conditions (O 2 flow rate = 0.6 mL min −1 and Rpq = 0.35), the new interferences of 96 Mo + and 96 Zr + could be oxidized to 96 Mo 16 O + and 96 Zr 16 O + , and reduced by up to 300-fold and 457-fold. The poor sensitivity of 80 Se 16 O + was increased 3.6-fold by introduced 2 mL min −1 CH 4 modifier to the ICP plasma. And a limit of quantification (LOQ, 10δ) of 0.06 μg L −1 was obtained. The accuracy of proposed method was validated by analysis of certified reference materials of trace elements in water (SRM 1643e) and trace elements in natural water (SRM 1640a), and the determined values were in good agreement with the certified values. The proposed method was also successfully applied for the determination of trace Se in Ca-rich groundwater samples, and the spiked recoveries was in the range of 90.0%–103%." @default.
- W2539929467 created "2016-11-04" @default.
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- W2539929467 date "2016-11-01" @default.
- W2539929467 modified "2023-09-24" @default.
- W2539929467 title "Determination of trace selenium in Ca-rich groundwater samples by ion molecule reaction ICP-MS and CH 4 plasma modifier" @default.
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- W2539929467 doi "https://doi.org/10.1016/j.ijms.2016.10.014" @default.
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