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- W2543897283 abstract "In the present study, the relationship between molecular structure and mechanical properties for a medium chain length polyhydroxyalkanoate (mcl-PHA) composed of 3-hydroxyoctanoate and 3-hydroxyhexanoate was elucidated. The mcl-PHA was crystallized from the melt at four different temperatures between its glass transition and melting point (37, 21, 3 and −21 °C) and its molecular structure was analysed by means of differential scanning calorimetry (DSC) and wide-angle X-ray diffractometry (WAXD). The mechanical properties, which were analysed via tensile-tests and dynamic mechanical analysis (DMA), were clearly affected by the selected crystallization temperature and corresponding molecular structure of the polymer. In this sense, samples crystallized at 37, 21 and 3 °C displayed higher secant moduli calculated at 2% (E2% ∼ 20 MPa) than the sample crystallized at −21 °C (E2% ∼ 7 MPa) due to their higher crystallinity. Even if samples crystallized at 37, 21 and 3 °C had very similar degree of crystallinity, their secant moduli calculated at 50, 100 and 200% (E50%, E100% and E200%) and yield strength (σy) were clearly affected by the selected crystallization temperature, showing a positive correlation (i.e., higher crystallization temperatures and corresponding more ordered crystalline domains with narrower crystal distributions resulted in higher E50%, E100% and E200% values)." @default.
- W2543897283 created "2016-11-04" @default.
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- W2543897283 date "2016-12-01" @default.
- W2543897283 modified "2023-10-18" @default.
- W2543897283 title "Effects of isothermal crystallization on the mechanical properties of a elastomeric medium chain length polyhydroxyalkanoate" @default.
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- W2543897283 doi "https://doi.org/10.1016/j.eurpolymj.2016.10.050" @default.
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