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• W2546677046 abstract "The synthesis and utilization of all carbon-chain ‘carbocontiguous’ azidoalkynyl precursors for an intramolecular click reaction is described. The substrates contain both azidoalkyl and ethynylmethyl groups which are conjoined by a 2-(phenylsulfonylmethyl)-4,5-diphenyloxazole lynchpin and are suitably disposed for ring closure. On promotion by copper salts, a number of cyclic click products having the 1,4-disubstituted endo-fused triazole component and the 4,5-diphenyloxazole component are obtained. In one case, removal of the phenylsulfonylmethyl group from the substrate prior to cyclization gave the 1,5-disubstituted exo-fused triazole. The utilization of CuSO4/sodium ascorbate system appears to be the optimal conditions for closure/cyclization and afforded the cyclized products in yields of 84–95%." @default.
• W2546677046 created "2016-11-11" @default.
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• W2546677046 date "2017-07-01" @default.
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• W2546677046 title "The intramolecular click reaction using ‘carbocontiguous’ precursors" @default.
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• W2546677046 doi "https://doi.org/10.1016/j.tet.2016.11.016" @default.
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