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- W2549112701 abstract "Four isostructural 3D lanthanide(iii) metal-organic frameworks with the general formula (H6edte)0.5[LnIII(ox)2(H2O)] (Ln = Gd (1), Tb (2), Dy (3) and Ho (4); H4edte = N,N,N',N'-tetrakis(2-hydroxyethyl)ethylenediamine) and ox = oxalate have been synthesized from oxalate. These compounds were characterized using single-crystal X-ray diffraction, FTIR and TGA/DTG. The magnetic investigation has been performed for 1-4 and the results reveal that a Gd(iii) containing MOF has the highest magnetic density and exhibits a larger cryogenic magnetocaloric effect (ΔSm = 35.9 J kg-1 K-1 for ΔH = 9 T at 2.0 K) with a high Debye temperature (θD = 342(3) and rD = 35). For the Dy derivative, an ac-out-of-phase signal was found, and further measurements under an applied field of 1000 Oe showed frequency-dependent out-of-phase magnetic susceptibility. Solid-state luminescence indicates that Tb and Dy-containing complexes are photoluminescent materials." @default.
- W2549112701 created "2016-11-30" @default.
- W2549112701 creator A5014181783 @default.
- W2549112701 creator A5046236467 @default.
- W2549112701 creator A5062973942 @default.
- W2549112701 creator A5079387142 @default.
- W2549112701 date "2017-01-01" @default.
- W2549112701 modified "2023-10-16" @default.
- W2549112701 title "3D oxalato-bridged lanthanide(<scp>iii</scp>) MOFs with magnetocaloric, magnetic and photoluminescence properties" @default.
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- W2549112701 doi "https://doi.org/10.1039/c6dt03843c" @default.
- W2549112701 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/27900384" @default.
- W2549112701 hasPublicationYear "2017" @default.
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