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- W2552224575 abstract "Abstract The electrochemical behavior of U(IV) in molten LiF–NaF–KF (46.5:11.5:42 mol) (FLINAK) eutectic salt was studied by cyclic voltammetry and square-wave voltammetry analyses. The reduction of U(IV) proceeded in two steps: reduction of initial U(IV) to U(III), followed by three-electron reduction of U(III) to U metal. Both reactions were reversible and controlled by ion diffusion at a scan rate of 0.02–0.3 V s −1 . A linear relationship between the reduction current density of U(III)/U(0) and the concentration of U(IV) was also established within 0.01–0.084 mol kg −1 . When different concentrations of Li 2 O were added to the FLINAK–UF 4 system, the peak current density of U(III)/U(0) was depleted because of the formation of UO 2 precipitates. The apparent solubility product ( Ksp ) of UO 2 in FLINAK–UF 4 –Li 2 O melts was approximately 4.75 × 10 −6 mol 3 /kg 3 , which can be used to evaluate the allowable amount of dissolved oxide ions in uranium-based fluorides." @default.
- W2552224575 created "2016-11-30" @default.
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- W2552224575 date "2016-12-01" @default.
- W2552224575 modified "2023-09-26" @default.
- W2552224575 title "Electrochemical technique for detecting the formation of uranium-containing precipitates in molten fluorides" @default.
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- W2552224575 doi "https://doi.org/10.1016/j.electacta.2016.11.135" @default.
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