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- W2552272511 abstract "Cu‐BTC–ethylenediamine (EDA)/polyethyleneimine (PEI) adsorbents were synthesized using a protophilic solvent‐assisted solvothermal method. EDA was introduced to enhance the degree of activation due to its lower boiling point allowing it to be removed easily compared with dimethylformamide. A contrast experiment was done by introducing PEI to the solvothermal solution considering its higher boiling point. Powder X‐ray diffraction, scanning electron microscopy and Raman spectroscopic characterizations were performed to investigate the effect of EDA/PEI on crystallinity and morphology of the adsorbents. 1 H NMR characterization and elemental analysis were performed to study the removal rate of organic guest molecules and the degree of activation. Nitrogen physical adsorption and CO 2 adsorption isotherms were used to measure the surface area and CO 2 adsorption capacities. The CO 2 adsorption mechanism of the synthesized adsorbents is mainly dependent on physisorption determined by surface area. Furthermore, open metal sites generated by the enhancement of degree of activation also promote the CO 2 adsorption performance. Therefore, adsorbents synthesized using the protophilic solvent‐assisted solvothermal method exhibit excellent CO 2 adsorption performance. Copyright © 2015 John Wiley & Sons, Ltd." @default.
- W2552272511 created "2016-11-30" @default.
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- W2552272511 date "2015-07-05" @default.
- W2552272511 modified "2023-10-16" @default.
- W2552272511 title "A protophilic solvent-assisted solvothermal approach to Cu-BTC for enhanced CO<sub>2</sub> capture" @default.
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- W2552272511 doi "https://doi.org/10.1002/aoc.3339" @default.
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