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• W2553519994 abstract "(E)-β-Iodoenamides and (E)-β-iodoenimides can be easily obtained from N-vinyl derivatives (N-vinylamides and N-vinylimides) by stereoselective ruthenium-catalysed silylative coupling with vinyltrimethylsilane (Marciniec coupling) and subsequent stereospecific silicon–iodine exchange. Bromodesilylation of (E)-β-silylenimides affords (E)-β-bromoenimides, while the analogous reactions involving (E)-β-silylenamides lead to decomposition of substrates. N-Halosuccinimides have been found as the most effective halogenating agents in the desilylation step under mild conditions. The ruthenium-catalysed silylation/halodesilylation sequence can be performed in a one-pot procedure. Copyright © 2015 John Wiley & Sons, Ltd." @default.
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• W2553519994 date "2015-02-08" @default.
• W2553519994 modified "2023-10-16" @default.
• W2553519994 title "A silicon-assisted synthesis of (E)-β-haloenamides fromN-vinylamides" @default.
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• W2553519994 doi "https://doi.org/10.1002/aoc.3284" @default.
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