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- W2554037996 abstract "A short synthesis of phenylethyl glycosides grayanoside-A 1, 2 and analogues 3-4 in high 43-65% overall yields is described. The main synthetic step involved regioselective O-6 acylation of unprotected 2-phenylethyl-β-D-glucoside 7 with cinnamoyl chlorides 8a-d using Me2SnCl2 as catalyst. The acylation at O-6 is regioselective regardless of the type of cinnamoyl chloride used. Protection/deprotection steps of the glucoside core were not necessary. The synthetic route is generally applicable for the synthesis of phenylpropanoid glycoside class of compounds acylated at O-6." @default.
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- W2554037996 date "2016-12-01" @default.
- W2554037996 modified "2023-10-16" @default.
- W2554037996 title "Short synthesis of phenylpropanoid glycoside grayanoside-A and analogues" @default.
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- W2554037996 doi "https://doi.org/10.1016/j.carres.2016.11.010" @default.
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