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- W2555633516 endingPage "e3670" @default.
- W2555633516 startingPage "e3670" @default.
- W2555633516 abstract "Treatment of Ru3(CO)12 with an equivalent of (2-phenyl-1H-inden-3-yl)dicyclohexylphosphine (1) and (2-pyridyl-1H-inden-1-yl)dicyclohexylphosphine (4) in refluxing heptane gave the novel trinuclear ruthenium clusters (μ3-η1:η2:η5–2-phenyl-3-Cy2PC9H4)Ru3(CO)8 (1c) and [μ2-η1–2-(pyridin-2-yl)-3-Cy2PC9H6]Ru3(CO)9 (4a), respectively, via C─H bond cleavage. (2-Mesityl-1H-inden-3-yl)dicyclohexylphosphine (2) reacted with Ru3(CO)12 in refluxing heptane to give the trinuclear ruthenium cluster [μ-2-mesityl-(3-Cy2PC9H5)](μ2-CO)Ru3(CO)9 (2c) via C─H bond cleavage and carbonyl insertion. 2-(Anthracen-9-yl)-1H–inden-3-yldicyclohexylphosphine (3) reacted with Ru3(CO)12 in refluxing heptane to give the dinuclear ruthenium cluster [μ2-η3:η3–2-(anthracen-9-yl)-3-Cy2PC9H6]Ru2(CO)5 (3a). The structures of 1c, 2c, 3a and 4a were fully characterized using IR and NMR spectroscopy, elemental analysis and single-crystal X-ray diffraction. These results suggest that the 2-aryl substituent on the indenyl ring has a pronounced effect on the reaction and coordination modes of Ru3(CO)12." @default.
- W2555633516 created "2016-11-30" @default.
- W2555633516 creator A5007294871 @default.
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- W2555633516 date "2016-11-10" @default.
- W2555633516 modified "2023-10-07" @default.
- W2555633516 title "Novel dinuclear and trinuclear ruthenium clusters derived from 2-aryl-substituted indenylphosphines via C─H bond cleavage" @default.
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- W2555633516 doi "https://doi.org/10.1002/aoc.3670" @default.
- W2555633516 hasPublicationYear "2016" @default.
- W2555633516 type Work @default.