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- W2561437892 abstract "Single crystals of dilithium‐acetylenedicarboxylate‐dihydrate, Li 2 ADC · 2H 2 O ( 1 ), were isolated from a solid product formed by isothermal evaporation of an aqueous solution of LiOH und acetylenedicarboxylic acid (H 2 ADC). 1 crystallizes in the triclinic space group P 1 with Z = 2. LiO 4 tetrahedra are interconnected by ADC 2– anions and water molecules to form a 3D polymeric structure. Coupled TGA and DTA measurements show that 1 loses its two water molecules above 100 °C. Heating a polycrystalline sample of 1 at 140 °C for 2 h in an argon atmosphere leads to a significant change of the powder diffraction pattern indicating the formation of the new anhydrous coordination polymer dilithium‐acetylenedicarboxylate, Li 2 ADC ( 2 ). Its crystal structure was solved and refined from X‐ray powder diffraction data. 2 crystallizes in the orthorhombic space group Fddd (Z = 8). LiO 4 tetrahedra are interconnected by ADC 2– anions to form a 3D polymeric structure." @default.
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- W2561437892 date "2016-11-15" @default.
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- W2561437892 title "Li<sub>2</sub>ADC·2H<sub>2</sub>O and Li<sub>2</sub>ADC: Two new Coordination Polymers with the Acetylenedicarboxylate Dianion (ADC<sup>2-</sup>)" @default.
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- W2561437892 doi "https://doi.org/10.1002/zaac.201600363" @default.
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