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• W2562088013 abstract "Abstract The rare-earth borosilicates RE 3 BSi 2 O 10 ( RE = Pr, Tb) were synthesized under high-temperature conditions of 1600 °C in a radio frequency furnace from praseodymium oxide, terbium oxide, silicon dioxide, silicon nitride, boron trioxide, and boric acid. The structure determinations based on powder diffraction data revealed that both phases RE 3 BSi 2 O 10 ( RE = Pr, Tb) are isotypic to Gd 3 BSi 2 O 10 [L. Chi, H. Chen, X. Lin, H. Zhuang, J. Huang, Jiegou Huaxue 1998 , 17 , 297]. The compounds crystallize in the orthorhombic space group Pbca (no. 61) with eight formula units and the lattice parameters a = 982.9(2), b = 714.2(2), c = 2314.4(4) pm, V = 1.6247(4) nm 3 , R p = 0.0231, and R wp = 0.0354 (all data) for Pr 3 BSi 2 O 10 and a = 960.5(5), b = 692.1(3), c = 2272.4(1) pm, V = 1.5106(2) nm 3 for Tb 3 BSi 2 O 10 . The lattice parameters of Tb 3 BSi 2 O 10 could be determined, but a final refinement of the powder data has not proved satisfactory. The structure of Pr 3 BSi 2 O 10 exhibits eight- (Pr1) and ninefold coordinated rare-earth cations (Pr2 and 3). Layers of ortho-silicate anions [SiO 4 ] 4– and borosilicate anions [BSiO 6 ] 5– are arranged alternatingly along the c axis and the RE cations are located in between." @default.
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• W2562088013 date "2015-11-17" @default.
• W2562088013 modified "2023-09-27" @default.
• W2562088013 title "Synthesis and structural characterization of the new rare-earth borosilicates Pr₃BSi₂O₁₀ and Tb₃BSi₂O₁₀" @default.
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• W2562088013 doi "https://doi.org/10.1515/znb-2015-0143" @default.
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