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• W2562803707 endingPage "974" @default.
• W2562803707 startingPage "968" @default.
• W2562803707 abstract "Abstract In this work we succeeded in synthesizing a chalcogenide glass, that is, the Ag 3 PS 4 glass, by milling the mixture of the crystalline Ag 2 S and P 2 S 5 powder. In terms of potential energy, the glass was excited by the milling process. The evidence for the energy excitation was the occurrence of the sub‐ T g relaxation recorded by a differential scanning calorimeter ( DSC ). The relaxation behavior in the milling‐derived Ag 3 PS 4 glass was found to significantly differ from that of a hyperquenched oxide glass. We observed two decoupled peaks of the energy release during a DSC scan, which are in contrast to the single asymmetric peak of the hyperquenched glass. The low‐temperature peak could be attributed to the β‐relaxation of the Ag–S ionic bonds, whereas the high‐temperature peak could arise from the α‐relaxation of the distorted rigid [ PS 4 ] units involving covalent bonds. The decoupling between the two peaks implies the fragile nature of the Ag 3 PS 4 glass. Upon the dynamic heating and the sub‐ T g annealing we found that the relaxation of the Ag 3 PS 4 glass is of high nonexponentiallity, and hence, of high structural heterogeneity." @default.
• W2562803707 created "2017-01-06" @default.
• W2562803707 creator A5036309567 @default.
• W2562803707 creator A5071477336 @default.
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• W2562803707 date "2016-12-21" @default.
• W2562803707 modified "2023-10-04" @default.
• W2562803707 title "Sub-<i>T</i> _g enthalpy relaxation in a milling-derived chalcogenide glass" @default.
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• W2562803707 doi "https://doi.org/10.1111/jace.14660" @default.
• W2562803707 hasPublicationYear "2016" @default.
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