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- W2562936732 abstract "The thesis dealt with the possible production of 1,3,5,7-tetranitro-1,3,5,7-tetrazocane (HMX). In theoretical part, literature survey is present and two promising methods are suggested for further investigation. Easy available hexamethylenetetramine is a starting material for both of the methods. The first procedure uses 1,5-diacetyl-3,7-dinitrotetrazocane (DADN) as an intermediate. Nitrolysis of DADN in nitric acid / phosphorus pentoxide mixture gives the best yield of HMX. The second procedure is based on nitrolysis by Bachmann method, in which starting hexamethylenetetramine is nitrolysed in one pot using acetic acid anhydride, acetic acid, paraformaldehyde, ammonium nitrate and urea based additives as a reaction medium. Both methods were modified to obtain the best yield of HMX. At the end of the work, the procedures are compared from economical point of view." @default.
- W2562936732 created "2017-01-06" @default.
- W2562936732 creator A5035833859 @default.
- W2562936732 date "2015-01-01" @default.
- W2562936732 modified "2023-09-23" @default.
- W2562936732 title "Příprava 1,3,5,7-tetranitro-1,3,5,7-tetrazokanu (HMX)" @default.
- W2562936732 hasPublicationYear "2015" @default.
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